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FUSION

Sample is fluxed with LiBorate/LiNO3 flux in automatic fusion equipment

Sample is fused in a Pt/Au crucible at 1050C and poured into Pt/Au mold

ANALYSIS

Zetium WD-XRF

LIMITATION

High Sulfide (S>10%) samples may not oxidize and fuse quantitatively


METHODXRF-LiB17
DIGESTLiBorate
WEIGHT0.5g
FINISHZetium WD-XRF
UNITS%
RANGELDL-UDL
1Al2O30.01-100XRF
2BaO0.01-60XRF
3CaO0.01-80XRF
4CeO2+XRF
5Cl+XRF
6Cr2O30.01-10XRF
7CuO+XRF
8Fe2O30.01-100XRF
9K2O0.01-15XRF
10La2O3+XRF
11MgO0.01-50XRF
12MnO0.01-39XRF
13MoO3+XRF
14Na2O0.01-20XRF
15NiO+XRF
16P2O50.01-40XRF
17SO30.01-30XRF
18SiO20.01-100XRF
19SnO2+XRF
20SrO0.01-2XRF
21ThO2+XRF
22TiO20.01-30XRF
23U3O8+XRF
24V2O50.01-10XRF
25WO3+XRF
26Y2O3+XRF
27ZnO0.01-10XRF
28ZrO20.01-20XRF
29LOI 1000C0.01-50Gravimetric
30C0.01-20ELTRA
Add-On Elements
aCeO20.01-20
bCl0.01-20
cCuO0.01-10
dLa2O30.01-20
eMoO30.01-10
fNiO0.01-10
gSnO20.01-10
hThO20.01-10
iU3O80.01-15
jWO30.01-10
kY2O30.01-10